反应条件
1: 1.) (COCl)2, 2.) AlCl3 / 1.) CH2Cl2, RT, 1 h, 2.) CS2, reflux, 30 min
2: 80 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature
3: PTSA / benzene / 0.5 h / Heating
4: DDQ / benzene / 0.17 h / Heating
View Scheme
参考文献
Amin, Shantu; Huie, Keith; Hussain, Nalband; Balanikas, George; Hecht, Stephen S.
Journal of Organic Chemistry, 1985 , vol. 50, # 11 p. 1948 - 1954
