N-(2-羟丙基)氨基甲酸叔丁酯合成路线 （共 7 条）
反应条件
in acetonitrile T=20°C; Condensation;
参考文献
Lew, Willard; Baskaran, Subramanian; Oslob, Johan D.; Yoburn, Joshua C.; Zhong, Min
Patent: US2006/35908 A1, 2006 ;
Location in patent: Page/Page column 108 ;
US 20060035908 A1
反应条件
in tetrahydrofuran T=60°C; 16 h;
参考文献
Menendez; Gotor
Synthesis, 1993 , # 1 p. 72 - 74
反应条件
1: 87 percent / hexane / 36 h / 60 °C / lipase from Candida antarctica 2: 84 percent / tetrahydrofuran / 16 h / 60 °C View Scheme
参考文献
Synthesis, , # 1 p. 72 - 74
反应条件
Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1298 - 1299
反应条件
potassium hydroxide; p-toluenesulfonyl chloride in tetrahydrofuran T=20 - 22°C;
参考文献
Kawamoto; Wills
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 16 p. 1916 - 1928
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; Inert atmosphereCooling with ice;
参考文献
Mai, Duy N.; Rosen, Brandon R.; Wolfe, John P.
Organic Letters, 2011 , vol. 13, # 11 p. 2932 - 2935
反应条件
1: 88 percent / pyridinium dichromate / dimethylformamide 2: 87.3 percent / HCO2H; Et3N / [Ru(II)(p-cymene)Cl2]2; (1R,2R)-TsDPEN / 24 h / 28 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 16 p. 1916 - 1928
