N,N’-双-(4-氯-苯基)-肼合成路线 （共 14 条）
反应条件
1: tin dichloride; alcohol; HCl / 0 °C / Das Hydrochlorid entsteht 2: 230 - 235 °C / neben anderen Produkten View Scheme
参考文献
Wilberg
Chemische Berichte, 1902 , vol. 35, p. 957 Anm.
反应条件
perchloric acid; lithium perchlorate in 1,4-dioxane; water T=0°C; different time; Product distributionMechanism;
参考文献
Rhee, Eun Sook; Shine, Henry J.
Journal of the American Chemical Society, 1986 , vol. 108, # 5 p. 1000 - 1006
参考文献
Calm; Heumann
Chemische Berichte, 1880 , vol. 13, p. 1181
反应条件
ammonium chloride; zinc in water; acetone
参考文献
Rhee, Eun Sook; Shine, Henry J.
Journal of the American Chemical Society, 1986 , vol. 108, # 5 p. 1000 - 1006
反应条件
triethylsilane; indium tribromide in N,N-dimethyl-formamide
T=60°C; 8 h;
参考文献
Sakai, Norio; Fujii, Kohji; Nabeshima, Shinya; Ikeda, Reiko; Konakahara, Takeo
Chemical Communications, 2010 , vol. 46, # 18 p. 3173 - 3175
反应条件
sodium dithionite; N,N'-dioctyl-4,4'-bipyridinium; potassium carbonate in water; acetonitrile
T=35°C; 2 h;
参考文献
Park, Kwanghee Koh; Han, Sun Young
Tetrahedron Letters, 1996 , vol. 37, # 37 p. 6721 - 6724
反应条件
sodium hydroxide; sodium tetrahydroborate; diphenylditellane in ethanol
15 h; Heating;
参考文献
Ohe, Kouichi; Uemura, Sakae; Sugita, Nobuyuki; Masuda, Hideki; Taga, Toru
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4169 - 4174
反应条件
hydrazine hydrate in ethanol
T=60°C; 0.5 h;
参考文献
Zhang, Chang-Rui; Wang, Yu-Lu
Synthetic Communications, 2003 , vol. 33, # 24 p. 4205 - 4208
反应条件
potassium hydroxide; aluminium in methanol
T=20°C; Reduction; Reductive coupling; 0.416667 h;
参考文献
Khurana, Jitender M.; Singh, Sarika
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 13 p. 1893 - 1895
反应条件
sodium tetrahydroborate; nickel boride in methanol
24 h; Ambient temperature;
参考文献
Nose, Atsuko; Kudo, Tadahiro
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 1529 - 1533
