1-苯甲基-1,4-二氢烟酰胺合成路线 (共 156 条)
反应条件
cis-[Ru(bpy)2(CO)(CHO)]PF6 in acetonitrile T=0°C; 0.25 h;
参考文献
Konno, Hideo; Sakamoto, Kazuhiko; Ishitani, Osamu
Angewandte Chemie, International Edition, 2000 , vol. 39, # 22 p. 4061 - 4063
Angewandte Chemie, 2000 , vol. 112, p. 4227 - 4229
反应条件
sodium dithionite; sodium carbonate in water T=20°C; 4 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 54, # 29 p. 3877 - 3881
反应条件
(OEP)Rh(III)Ac in isopropyl alcohol; acetonitrile; benzene T=15°C; 9 h; Irradiation;
参考文献
Aoyama, Yasuhiro; Midorikawa, Koji; Toi, Hiroo; Ogoshi, Hisanobu
Chemistry Letters, 1987 , p. 1651 - 1654
反应条件
1: 64 percent / methanol; dioxane / 5 h / 80 °C 2: 82 percent / sodium carbonate; sodium dithionite / H2O / 2 h View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 689, # 25 SPEC. ISS. p. 4783 - 4790
反应条件
1: With sodium carbonate in water T=20°C; Inert atmosphere; 2: With sodium dithionite in water 4 h; Inert atmosphere;
参考文献
Haynes, Richard K.; Chan, Wing-Chi; Wong, Ho-Ning; Li, Ka-Yan; Wu, Wai-Keung; Fan, Kit-Man; Sung, Herman H. Y.; Williams, Ian D.; Prosperi, Davide; Melato, Sergio; Coghi, Paolo; Monti, Diego
ChemMedChem, 2010 , vol. 5, # 8 p. 1282 - 1299
反应条件
ascorbic acid powder; [Ru(2,2′-bipyridine)3]2+; Rh(I)HCl(P(Ph)2(C6H4SO3-))34- in water Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 4 p. 559 - 564
反应条件
1-benzyl-1,2-dihydroisonicotinamide in methanol 0.0833333 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 3245 - 3256
反应条件
1-benzyl-3-carbamoylpyridinium hexafluorophosphate in acetonitrile 16 h; Ambient temperature;
参考文献
Anne; Moiroux
Canadian Journal of Chemistry, 1995 , vol. 73, # 4 p. 531 - 538
反应条件
1: ethanol / 6 h / Heating 2: Na2S2O4, carbonate / H2O View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 12 p. 2053 - 2056
反应条件
sodium dithionite; sodium carbonate in water
参考文献
Pavlikova-Raclova, Frantiska; Kuthan, Josef
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1408 - 1421