5-甲氧基-4,7-菲咯啉合成路线 （共 10 条）
反应条件
sulfuric acid; nitric acid T=96°C; 2 h;
参考文献
Bonhote, Pierre; Wrighton, Mark S.
Synlett, 1997 , vol. 1997, # 8 p. 897 - 898
参考文献
Eistert,B.; Fink,G.
Chemische Berichte, 1962 , vol. 95, p. 2395 - 2402
Full Text Show Details
Druey; Schmidt
Helvetica Chimica Acta, 1950 , vol. 33, p. 1080,1085
反应条件
sulfuric acid; m-nitrobenzene sulfonic acid sodium salt in water
6 h; Heating;
参考文献
Imor, Susan; Morgan, Robert J.; Wang, Sihe; Morgan, Oma; Baker
Synthetic Communications, 1996 , vol. 26, # 11 p. 2197 - 2203
反应条件
diarsenic pentoxide; sulfuric acid; glycerol
参考文献
CIBA
Patent: DE834996 , 1951 ;
DRP/DRBP Org.Chem.
Full Text Show Details
CIBA
Patent: US2640830 , 1950 ;
反应条件
potassium hydroxide; copper
T=180°C;
参考文献
CIBA
Patent: US2640830 , 1950 ;
反应条件
sulfuric acid; glycerol
参考文献
Eistert,B.; Fink,G.
Chemische Berichte, 1962 , vol. 95, p. 2395 - 2402
Full Text Show Details
Druey; Schmidt
Helvetica Chimica Acta, 1950 , vol. 33, p. 1080,1085
Full Text Show Details
CIBA
Patent: US2640830 , 1950 ;
反应条件
1: Raney nickel; ethanol / Hydrogenation
2: glycerol; aqueous H2SO4
View Scheme
参考文献
CIBA
Patent: US2640830 , 1950 ;
反应条件
sulfuric acid; sodium o-nitrobenzenesulfonate
1) 98 deg C, 1 h then 140 deg C, 1 h, 2) 70 - 90 deg C then 133 deg C, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bonhote, Pierre; Wrighton, Mark S.
Synlett, 1997 , vol. 1997, # 8 p. 897 - 898
反应条件
2: methanol. KOH; copper-powder / 180 °C
View Scheme
参考文献
CIBA
Patent: US2640830 , 1950 ;
参考文献
Terent'ev, P. B.; Stankyavichyus, A. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 11 p. 1258 - 1262
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 11 p. 1518 - 1521
