N-甲氧基-N-甲基-2-呋喃甲酰胺合成路线 （共 13 条）
反应条件
pyridine; sodium carbonate in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Franchi, Luigi; Rinaldi, Marta; Vignaroli, Giulia; Innitzer, Anna; Radi, Marco; Botta, Maurizio
Synthesis, 2010 , # 22 art. no. Z19310SS, p. 3927 - 3933
反应条件
1: in dichloromethane T=18°C; 0.25 h; 2: With tributylphosphine; (2-pyridine-N-oxide)disulfide in dichloromethane
参考文献
Banwell; Smith
Synthetic Communications, 2001 , vol. 31, # 13 p. 2011 - 2019
反应条件
dimethylaluminum chloride in hexane; dichloromethane 0.5 h; Ambient temperature;
参考文献
Shimizu, Takeshi; Osako, Katsuhisa; Nakata, Tadashi
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2685 - 2688
参考文献
Niu, Teng; Zhang, Weiming; Huang, Danfeng; Xu, Changming; Wang, Haifeng; Hu, Yulai
Organic Letters, 2009 , vol. 11, # 19 p. 4474 - 4477
反应条件
pyridine in dichloromethane
参考文献
Gebauer, Julian; Dewi, Purnama; Blechert, Siegfried
Tetrahedron Letters, 2005 , vol. 46, # 1 p. 43 - 46
反应条件
triethylamine Acylation;
参考文献
Barrett, Anthony G. M.; Cramp, Susan M.; Roberts, Richard S.; Zecri, Frederic J.
Organic Letters, 2000 , vol. 2, # 3 p. 261 - 264
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C / |Inert atmosphere 2: triethylamine / dichloromethane / 2 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 16 p. 3316 - 3327
反应条件
1: n-bromopentane With magnesium in diethyl ether 1 h; Heating / reflux; 2: N-methoxy-N-methyl-2-pyrrolecarboxamide in diethyl ether T=0°C; 3 h; 3: With hydrogenchloride in diethyl ether; water T=0°C;
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US7161015 B1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide T=100°C;
参考文献
Cutulic, Sylvain P. Y.; Murphy, John A.; Farwaha, Hardeep; Zhou, Sheng-Ze; Chrystal, Ewan
Synlett, 2008 , # 14 p. 2132 - 2136
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=-40 - -15°C; 2: N-methoxy-N-methyl-2-pyrrolecarboxamide in tetrahydrofuran; hexane T=-78 - 22°C;
参考文献
Friel, Donna K.; Snapper, Marc L.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2008 , vol. 130, # 30 p. 9942 - 9951
