4-氨基-2,6-二-叔丁基苯酚合成路线 （共 12 条）
反应条件
hydrogen; palladium on activated carbon in ethanol; dichloromethane T=30°C; P=1034.32 Torr; 2 h;
参考文献
Societe de Conseils de Recherches et d'Applications Scientifiques (S.C.R.A.S.)
Patent: US6340700 B1, 2002 ;
Location in patent: Page column 33 ;
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; P=760.051 Torr;
参考文献
Shekhovtsov, Sergey V.; Omelchenko, Irina V.; Dyakonenko, Viktoriya V.; Shishkin, Oleg V.; Allmann, Rudolf; Libor, Thomas; Reichardt, Christian; McHedlov-Petrossyan, Nikolay O.
Dyes and Pigments, 2012 , vol. 92, # 3 p. 1394 - 1399
反应条件
2: H2 / Raney-Ni View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 8, p. 469 - 474
参考文献
Justus Liebigs Annalen der Chemie, , vol. 661, p. 1 - 37
Journal of Medicinal Chemistry, , vol. 8, p. 469 - 474
反应条件
1: 95 percent / 2 h / 180 - 185 °C 2: acid hydrolysis View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2184 - 2185
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2356 - 2358
反应条件
1: 16.2 percent / chromic anhydride 2: hydroxylamine 3: 5percent sodium hydroxide, sodium dithionite / 45 - 60 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, # 7 p. 1934 - 1942
反应条件
acid hydrolysis; Yield given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2184 - 2185
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2356 - 2358
反应条件
1: 2 h / 180 - 185 °C 2: acid hydrolysis View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2184 - 2185
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2356 - 2358
反应条件
1: 2 h / 180 - 185 °C 2: acid hydrolysis View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2184 - 2185
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2356 - 2358
反应条件
in methanol T=20°C; 0.5 h;
参考文献
Alisi, Maria Alessandra; Brufani, Mario; Cazzolla, Nicola; Ceccacci, Francesca; Dragone, Patrizia; Felici, Marco; Furlotti, Guido; Garofalo, Barbara; La Bella, Angela; Lanzalunga, Osvaldo; Leonelli, Francesca; Marini Bettolo, Rinaldo; Maugeri, Caterina; Migneco, Luisa Maria; Russo, Vincenzo
Tetrahedron, 2012 , vol. 68, # 49 p. 10180 - 10187
