反应条件
in toluene Ce(O-i-Pr)4 is dissolved in toluene, soln. of n-Bu3SnCp is added, mixt. is heated at 65°C for 24 h (N2); mixt. is cooled to room temp., filtn., volatile components are removed under high vac., recrystn. at -78°C (pentane) or sublimation at 70°C (10E-5 Torr); elem. anal.;
参考文献
Gulino, Antonio; Casarin, Maurizio; Conticello, Vincent P.; Gaudiello, John G.; Mauermann, Heiko; et al.
Organometallics, 1988 , vol. 7, p. 2360 - 2364