Fukuzumi, Shunichi; Kotani, Hiroaki; Prokop, Katharine A.; Goldberg, David P.
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1859 - 1869
diphenylphosphinic oxide; oxygen in acetonitrile T=20°C; 0.333333 h; Irradiationother times; also without methanol; also under an Ar atmosphere; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2099 - 2105
in acetonitrile 1 h; Irradiationalso in the presence of var. amount of iodine or tetrabutylammonium iodide, also in the presence air, also 10-methylacridinium tetrafluoroborate; MechanismProduct distribution;
in water byproducts: CO; React. of starting materials in H2O under N2 or Ar atmosphere.; Evolution of CO obsd. (gas chromy.). Filtn. of pptd. colorless solid, washing with H2O and drying (vac.) over P4O10 gives org. compd. Extn. of aq. soln. (Et2O), evapn. of combined ether ext. to dryness under reduced pressure, IR spectoscopy.;
