甲基-1-羟基-2-萘甲酸盐合成路线 (共 73 条)
反应条件
1: ethyl phenylsulphonylacetate With sodium hydride in tetrahydrofuran T=20°C; 0.166667 h; 2: o-(trimethylsilyl)phenyl triflate; acrylic acid methyl ester With potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=65°C; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 72, # 10 p. 3965 - 3968
反应条件
in diethyl ether; dichloromethane T=-78°C;
参考文献
Journal of the American Chemical Society, , vol. 135, # 17 p. 6633 - 6642
参考文献
Alonso, Miguel E.; Chitty, A. Wladimir; Pekerar, Sarah; Borgo, Maria de L.
Journal of the Chemical Society, Chemical Communications, 1984 , # 22 p. 1542 - 1543
反应条件
1: petroleum ether; thionyl chloride View Scheme
参考文献
Journal of the Chemical Society, , p. 309
反应条件
in tetrahydrofuran 2 h; Ambient temperature; Yields of byproduct given;
参考文献
Organic Mass Spectrometry, , vol. 24, p. 1043 - 1044
参考文献
Journal of the Indian Chemical Society, , vol. 13, p. 645,648
Journal of the Chemical Society, , p. 309
参考文献
Journal of the Chemical Society, , vol. 97, p. 1747
参考文献
Chemische Berichte, , vol. 57, p. 1290
反应条件
lithium tert-butylate multistep reaction: 1) THF, -60 deg C, 15 - 20 min; 2) THF, -60 deg C, 3 h; further Michael acceptors and thiophthalides; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 309 - 316
参考文献
Chemische Berichte, , vol. 20, p. 2700