甲基-1-羟基-2-萘甲酸盐合成路线 (共 73 条)
反应条件
1: 2-mercaptoacetic acid methyl ester With potassium in methanol 2: methyl 2-[2-(1,1,1-trimethylsilyl)-1-ethynyl] benzoate in methanol Microwave irradiation;
参考文献
Cikotiene, Inga; Buksnaitiene, Rita; Sazinas, Rokas
Tetrahedron, 2011 , vol. 67, # 4 p. 706 - 717
反应条件
C10H12INO4 in chloroform; diethylene glycol dimethyl ether; water T=40°C; 24 h;
参考文献
Cui, Li-Qian; Dong, Zhi-Lei; Liu, Kai; Zhang, Chi
Organic Letters, 2011 , vol. 13, # 24 p. 6488 - 6491
反应条件
lithium hydroxide in tetrahydrofuran Methylation; esterification; 1 h; Heating;
参考文献
Chakraborti, Asit K.; Basak, Anindita; Grover, Vikas
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 8014 - 8017
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in N,N-dimethyl-formamide T=100°C; P=30400 Torr; 10 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
methanol; bis-triphenylphosphine-palladium(II) chloride; triethylamine in N,N-dimethyl-formamide T=100°C; P=30400 Torr; 10 h; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
C10H12INO4; water in o-di-fluorobenzene; diethylene glycol dimethyl ether T=40°C; 24 h;
参考文献
Organic Letters, , vol. 13, # 24 p. 6488 - 6491
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in N,N-dimethyl-formamide T=100°C; P=30400 Torr; 10 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
oxygen; methylene blue in methanol Ambient temperatureIrradiation;
参考文献
Tetrahedron Letters, , vol. 32, # 11 p. 1471 - 1474
反应条件
boron trichloride in dichloromethane T=25°C; 15 h;
参考文献
Piccolo, Oreste; Filippini, Lucio; Tinucci, Laura; Valoti, Ermanno; Citterio, Attilio
Tetrahedron, 1986 , vol. 42, # 3 p. 885 - 892
反应条件
oxygen in methanol T=30°C; P=760.051 Torr;
参考文献
Chemistry Letters, , vol. 41, # 9 p. 976 - 978