3-(2-吡啶)-[1,2,3]噻唑并[1,5-a]吡啶合成路线 (共 9 条)
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); para-iodoanisole in N,N-dimethyl-formamide T=65°C; 24 h;
参考文献
Abarca, Belen; Ballesteros, Rafael; Blanco, Fernando; Bouillon, Alexandre; Collot, Valerie; Dominguez, Jose-Reynaldo; Lancelot, Jean-Charles; Rault, Sylvain
Tetrahedron, 2004 , vol. 60, # 22 p. 4887 - 4893
反应条件
hydrazine hydrate in methanol; water 4 h; Heating;
参考文献
Battaglia, Luigi P.; Carcelli, Mauro; Ferraro, Fabrizio; Mavilla, Luigi; Pelizzi, Corrado; Pelizzi, Giancarlo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 18 p. 2651 - 2654
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in 1,4-dioxane T=85°C; Suzuki cross-coupling reaction;
参考文献
Tetrahedron Letters, , vol. 47, # 46 p. 8101 - 8103
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=140°C; 2 h; Inert atmosphere;
参考文献
Arkivoc, , vol. 2012, # 9 p. 229 - 241
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=140°C; 2 h; Inert atmosphere;
参考文献
Arkivoc, , vol. 2012, # 9 p. 229 - 241
反应条件
1: iodine; potassium hydroxide / dimethylformamide 2: aq. sodium carbonate; Pd(PPh3)4 / dioxane / 85 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 47, # 46 p. 8101 - 8103
反应条件
1: 1.) LDA / 1.) THF, hexane, -40 deg C, 4 h, 2.) THF, hexane, CH2Cl2, rt, overnight 2: 90 percent / SeO2 / aq. H2SO4 / 10 h / Heating View Scheme
参考文献
Abarca, Belen; Ballesteros, Rafael; Elmasnaouy, Mostafa
Tetrahedron, 1998 , vol. 54, # 50 p. 15287 - 15292
反应条件
palladium 10 on activated carbon; zinc in ethanol T=150°C; 24 h; Autoclave; Reagent/catalyst;
参考文献
Abarca, Belen; Adam, Rosa; Alom, Shamim; Ballesteros, Rafael; Lopez-Molina, Sonia
Arkivoc, 2014 , vol. 2014, # 2 p. 175 - 186
反应条件
palladium 10 on activated carbon; zinc in ethanol; water T=150°C; 24 h; Autoclave;
参考文献
Arkivoc, , vol. 2014, # 2 p. 175 - 186