lithium methanolate in methanol; N,N-dimethyl-formamide
T=90°C; 4.5 h;
参考文献
Hewgill, Frank R.; Slamet, Riskiono; Stewart, Jeffery M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3033 - 3042
1: 67 percent / toluene / 45 h / 60 °C
2: 82 percent / LiOMe / dimethylformamide; methanol / 4.5 h / 90 °C
View Scheme
参考文献
Hewgill, Frank R.; Slamet, Riskiono; Stewart, Jeffery M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3033 - 3042
1: 95 percent / thionyl chloride, pyridine / CH2Cl2 / 0.5 h
2: 67 percent / toluene / 45 h / 60 °C
3: 82 percent / LiOMe / dimethylformamide; methanol / 4.5 h / 90 °C
View Scheme
参考文献
Hewgill, Frank R.; Slamet, Riskiono; Stewart, Jeffery M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3033 - 3042
