反应条件
1: 1.) 80 percent arsenic acid, CuO, 2.) conc. HCl / 1.) H2O, 70 deg C, 2 h, 2.) CCl4, 5 min
2: 9 percent / PhLi / tetrahydrofuran; benzene; diethyl ether / 1.) -120 deg C, 2.) -120 deg C to r.t.
View Scheme
参考文献
Kauffmann, Thomas; Altepeter, Bruno; Klas, Norbert; Kriegesmann, Reinhard
Chemische Berichte, 1985 , vol. 118, # 6 p. 2353 - 2364