3,5-二氯-2-羟基-4-甲氧基-6-丙基苯甲酸合成路线 （共 15 条）
反应条件
1: 88 percent / BCl3 / CH2Cl2
2: 98 percent / SO2Cl2 / 3 h / Ambient temperature
3: 37 percent / NaOH/H2O / ethanol / 18 h / Heating
View Scheme
参考文献
Green, Richard H.
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4697 - 4700
反应条件
1: 81 percent / K2CO3 / acetone / 3 h / Heating
2: 88 percent / BCl3 / CH2Cl2
3: 98 percent / SO2Cl2 / 3 h / Ambient temperature
4: 37 percent / NaOH/H2O / ethanol / 18 h / Heating
View Scheme
参考文献
Green, Richard H.
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4697 - 4700
反应条件
1: NaClO2, NH3SO3H / tetrahydrofuran; H2O / 5.5 h / Ambient temperature
2: NaOH/H2O / ethanol / 0.75 h / Ambient temperature
View Scheme
参考文献
Green, Richard H.
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4697 - 4700
反应条件
1: 70 percent Turnov. / K2CO3 / acetone / 5 h
2: 61 percent / sulfuryl chloride / 0.17 h / Ambient temperature
3: 33 percent / conc. H2SO4 / 12 h / Ambient temperature
View Scheme
参考文献
Mori, Kenji; Kamada, Atsushi; Mori, Hideto
Liebigs Annalen der Chemie, 1989 , p. 303 - 306
反应条件
1: 61 percent / sulfuryl chloride / 0.17 h / Ambient temperature
2: 33 percent / conc. H2SO4 / 12 h / Ambient temperature
View Scheme
参考文献
Mori, Kenji; Kamada, Atsushi; Mori, Hideto
Liebigs Annalen der Chemie, 1989 , p. 303 - 306
