4-甲基-6-十六酰氨基香豆素-β-D-吡喃半乳糖苷合成路线 （共 6 条）
反应条件
sodium methylate in methanol; acetonitrile
T=20°C; 36 h;
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 5 p. 496 - 499
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 5 p. 603 - 606
反应条件
1: 62 percent / dimethylsulfoxide; tetrahydrofuran / 22 h / Heating
2: 58 percent / Sodium methanolate / methanol; acetonitrile / 36 h / 20 °C
View Scheme
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 5 p. 496 - 499
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 5 p. 603 - 606
反应条件
1: 62 percent / dimethylsulfoxide; tetrahydrofuran / 22 h / Heating
2: 58 percent / Sodium methanolate / methanol; acetonitrile / 36 h / 20 °C
View Scheme
参考文献
Kozlova, I. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 5 p. 496 - 499
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 5 p. 603 - 606
反应条件
1: 90 percent / pyridine / 3 h / 20 °C
2: 1) sodium ethoxide / 1) ethanol, 2) DMSO, oxolane, 20h, reflux
3: sodium methoxide
View Scheme
参考文献
Wiederschain, German Ya.; Kozlova, Inna K.; Ilyina, Galina S.; Mikhaylova, Margarita A.; Beyer, Elena M.
Carbohydrate Research, 1992 , vol. 224, p. 255 - 272
反应条件
1: 1) sodium ethoxide / 1) ethanol, 2) DMSO, oxolane, 20h, reflux
2: sodium methoxide
View Scheme
参考文献
Wiederschain, German Ya.; Kozlova, Inna K.; Ilyina, Galina S.; Mikhaylova, Margarita A.; Beyer, Elena M.
Carbohydrate Research, 1992 , vol. 224, p. 255 - 272
反应条件
1: 90 percent / pyridine / 3 h / 20 °C
2: 1) sodium ethoxide / 1) ethanol, 2) DMSO, oxolane, 20h, reflux
3: sodium methoxide
View Scheme
参考文献
Wiederschain, German Ya.; Kozlova, Inna K.; Ilyina, Galina S.; Mikhaylova, Margarita A.; Beyer, Elena M.
Carbohydrate Research, 1992 , vol. 224, p. 255 - 272
