2,6-二甲氧基乙酸苯酯合成路线 （共 11 条）
反应条件
1: AlCl3; nitrobenzene 2: aqueous HCl; amalgamated zinc View Scheme
参考文献
Pepper; Hibbert
Journal of the American Chemical Society, 1948 , vol. 70, p. 67,70
反应条件
1: 1.05 g / Cl2 / acetic acid / 1 h / 20 °C 2: 220 mg / NaOH / methanol / 1 h / 40 °C View Scheme
参考文献
Smith; Wearne; Wallis
Chemosphere, 1994 , vol. 28, # 5 p. 921 - 930
反应条件
potassium dichromate; sulfuric acid; acetic acid
参考文献
Graebe; Hess
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 239
反应条件
bismuth trifluoromethanesulphonate in toluene Fries rearrangement; 1 h; Heating;
参考文献
Sreedhar; Swapna; Sridhar
Synthetic Communications, 2004 , vol. 34, # 8 p. 1433 - 1440
反应条件
tetrabutyl-ammonium chloride; sodium hydroxide in dichloromethane; water
T=0°C; 0.0833333 h;
参考文献
Simion, Alina Marieta; Hashimoto, Iwao; Mitoma, Yoshiharu; Egashira, Naoyoshi; Simion, Cristian
Synthetic Communications, 2012 , vol. 42, # 6 p. 921 - 931
反应条件
dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid
T=80°C; Baeyer-Villiger oxidation; 1 h;
参考文献
Bjorsvik, Hans-Rene; Occhipinti, Giovanni; Gambarotti, Cristian; Cerasino, Leonardo; Jensen, Vidar R.
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7290 - 7296
参考文献
Brand; Collischonn
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 103, p. 344,349
参考文献
Brand; Collischonn
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 103, p. 344,349
反应条件
zinc(II) chloride
T=120°C;
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1928 , vol. <2> 118, p. 316
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 121, p. 256
反应条件
1: 1.40 g / Cl2 / acetic acid / 1 h / 20 °C
2: 720 mg / NaOCH3 / methanol / 1 h / 40 °C
View Scheme
参考文献
Smith; Wearne; Wallis
Chemosphere, 1994 , vol. 28, # 5 p. 921 - 930
