苄基-(3,4,5-三甲氧基苄基)胺合成路线 （共 6 条）
反应条件
sodium tetrahydroborate; sodium hydroxide in methanol; water
T=60 - 70°C;
参考文献
Rani, Neeraj; Sharma; Kaul; Manrao
Journal of the Indian Chemical Society, 2008 , vol. 85, # 10 p. 1041 - 1044
反应条件
ethanol; nickel
T=100°C; P=73550.8 Torr; Hydrogenation;
参考文献
Adorni; Ishii
Anales de la Asociacion Quimica Argentina (1921-2001), 1945 , vol. 33, p. 71,75
反应条件
polymer supported cyanoborohydride in methanol; toluene
72 h; Ambient temperature; Yield given;
参考文献
Ley, Steven V.; Bolli, Martin H.; Hinzen, Berthold; Gervois, Anne-Geraldine; Hall, Beverley J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 15 p. 2239 - 2241
反应条件
1: benzene
2: Raney nickel; ethanol / 100 °C / 73550.8 Torr / Hydrogenation
View Scheme
参考文献
Adorni; Ishii
Anales de la Asociacion Quimica Argentina (1921-2001), 1945 , vol. 33, p. 71,75
反应条件
1: benzene
2: Raney nickel; ethanol / 100 °C / 73550.8 Torr / Hydrogenation
View Scheme
参考文献
Adorni; Ishii
Anales de la Asociacion Quimica Argentina (1921-2001), 1945 , vol. 33, p. 71,75
反应条件
sodium tetrahydroborate
1.) methanol, dioxane, 20 min, r.t.; 2.) methanol, dioxane, 20 min, 0 deg C; Yield given. Multistep reaction;
参考文献
Simig; Fetter; Hornyak; et al.
Acta Chimica Hungarica, 1985 , vol. 119, # 1 p. 17 - 32
