4,5-二氯邻苯二甲酸酐合成路线 （共 38 条）
反应条件
acetic anhydride 2 h; Heating;
参考文献
Caswell; Guevara; Corley; Martinez; Hollis; Largess; Thornley
Synthesis, 1992 , # 9 p. 823 - 825
参考文献
Occidental Chemical Corporation
Patent: US5059697 A1, 1991 ;
反应条件
alkaline solution; chlorine in Gegenwart von Antimon-Salzen;
参考文献
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 7, p. 1113
Chem. Zentralbl., , vol. 107, # II p. 2901
反应条件
chlorine T=390°C; var. temp, var. conc. of Cl2; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 48, # 15 p. 2465 - 2468
参考文献
Chemische Berichte, , vol. 42, p. 3533
反应条件
1: 47 percent / formamide / 2 h / 150 °C 2: 45 percent / Sn/HCl / 4 h / Heating View Scheme
参考文献
Hennige, Hans; Kreher, Richard P.; Konrad, Michael; Jelitto, Frank
Chemische Berichte, 1988 , vol. 121, p. 243 - 252
反应条件
1: With sodium methylate in methanol 12 h; Heating / reflux; 2: With hydrogenchloride in methanol; water
参考文献
Allison, Brett; Phuong, Victor K.; Pippel, Marna C.W.; Rabinowitz, Michael H.; Venkatesan, Hariharan
Patent: US2006/69286 A1, 2006 ;
Location in patent: Page/Page column 19 ;
US 20060069286 A1
反应条件
1: in methanol T=0 - 20°C; 3 h; 2: With hydrogenchloride in water
参考文献
Pippel, Marna; Boyce, Kristen; Venkatesan, Hariharan; Phuong, Victor K.; Yan, Wen; Barrett, Terrance D.; Lagaud, Guy; Li, Lina; Morton, Magda F.; Prendergast, Clodagh; Wu, Xiaodong; Shankley, Nigel P.; Rabinowitz, Michael H.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 22 p. 6376 - 6378
参考文献
Liu, Jing; Deng, Xiaohu; Fitzgerald, Anne E.; Sales, Zachary S.; Venkatesan, Hariharan; Mani, Neelakandha S.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 8 p. 2654 - 2660
反应条件
1: 98 percent / formamide / 3 h / Heating 2: 72 percent / 25-33percent NH4OH / 48 h / Ambient temperature 3: 75 percent / SOCl2, DMF / 1) 0 - 5 deg C, 5 h, 2) r.t., 24 h 4: 59 percent / K2CO3 / dimethylsulfoxide / 0.5 h / 90 °C View Scheme
参考文献
Wohrle; Eskes; Shigehara; Yamada
Synthesis, 1993 , # 2 p. 194 - 196
