4-(1,1-二甲基乙基)苯甲酸丁酯合成路线 （共 7 条）
反应条件
4 A molecular sieve; potassium carbonate; palladium diacetate in toluene
T=100°C; P=760.051 Torr; 15 h;
参考文献
Munday, Rachel H.; Martinelli, Joseph R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 9 p. 2754 - 2755
反应条件
4 A molecular sieve; potassium carbonate; palladium diacetate in toluene
T=100°C; P=760.051 Torr; 15 h;
参考文献
Munday, Rachel H.; Martinelli, Joseph R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 9 p. 2754 - 2755
反应条件
4 A molecular sieve; potassium carbonate; palladium diacetate in toluene
T=100°C; P=760.051 Torr; 15 h;
参考文献
Munday, Rachel H.; Martinelli, Joseph R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 9 p. 2754 - 2755
反应条件
copper(l) iodide; 1,10-phenanthroline in o-xylene
T=150°C; 6 h; Inert atmosphere;
参考文献
Nakatani, Yuji; Koizumi, Yuichiro; Yamasaki, Ryu; Saito, Shinichi
Organic Letters, 2008 , vol. 10, # 10 p. 2067 - 2070
反应条件
water; tetra-(n-butyl)-phosphonium bromide in chlorobenzene
T=100°C; also in the presence of dicyclohexano-18-crown-6; Rate constant;
参考文献
Dehmlow, Eckehard V.; Raths, Hans-Christian
Journal of Chemical Research, Miniprint, 1988 , # 12 p. 2901 - 2917
反应条件
in methanol-d4
T=34.9°C; Ea, ΔS(excit.), other N-acetoxy-O-butyl benzohydroxamates; Rate constantThermodynamic dataMechanism;
参考文献
Campbell, John J.; Glover, Stephen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 10 p. 1661 - 1663
反应条件
in methanol-d4
T=34.85°C; Rearrangement; KineticsActivation energy; Further Variations:Temperatures;
参考文献
Campbell, John J.; Glover, Stephen A.
Journal of Chemical Research, Miniprint, 1999 , # 8 p. 2075 - 2096
