3-溴-1-甲基-1H-喹啉-2-酮合成路线 （共 7 条）
反应条件
potassium hydroxide in methanol T=20°C; 3 h;
参考文献
Franck, Philippe; Hostyn, Steven; Dajka-Halasz, Beata; Polonka-Balint, Agnes; Monsieurs, Katrien; Matyus, Peter; Maes, Bert U.W.
Tetrahedron, 2008 , vol. 64, # 26 p. 6030 - 6037
反应条件
1: 55 percent / TsCl, K2CO3 / CHCl3 / 6 h / Ambient temperature 2: 81 percent / K2CO3 / dimethylformamide / 3 h / 60 °C View Scheme
参考文献
Synlett, , vol. 1997, # 9 p. 1067 - 1068
反应条件
1.1: toluene / 48 h / 20 °C / Inert atmosphere 2.1: tetrahydrofuran / 6 h / -10 - 20 °C / Inert atmosphere 2.2: 0.5 h / 20 °C / Inert atmosphere 3.1: water View Scheme
参考文献
Tetrahedron, , vol. 67, # 3 p. 655 - 659
反应条件
1.1: tetrahydrofuran / 6 h / -10 - 20 °C / Inert atmosphere 1.2: 0.5 h / 20 °C / Inert atmosphere 2.1: water View Scheme
参考文献
Tetrahedron, , vol. 67, # 3 p. 655 - 659
反应条件
1: 2-methyl-propan-2-ol / 0.25 h / Irradiation 2: air, SiO2 / CHCl3 / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 25, # 19 p. 2999 - 3006
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 45, p. 179
Chemische Berichte, , vol. 36, p. 1206
反应条件
1: 85 percent / NaHCO3 / Pd(0) / 1,2-dimethoxy-ethane; H2O / 3 h
2: 100 percent / 20percent H2SO4 / ethanol / 48 h / Heating
3: 65 percent / POCl3 / benzene / 3 h / Heating
View Scheme
参考文献
Timari, Geza; Soos, Tibor; Hajos, Gyoergy
Synlett, 1997 , vol. 1997, # 9 p. 1067 - 1068
