diisobutylaluminium hydride in hexane; toluene T=-68°C; 2 h;

chloramine-T in 1,4-dioxane; water 1 h;

暂无反应条件数据

1: 1.) Na-N-methylanilide 2.) isoamyl nitrite / 1.) ether, -78 deg C, 0,5h 2.) THF, -10 deg C, 1h 2: 83 percent / acetic anhydride, glacial acetic acid / 3 h / 80 °C 3: 43 percent / diisobutylaluminum hydride / toluene; hexane / 2 h / -68 °C View Scheme

1: 83 percent / acetic anhydride, glacial acetic acid / 3 h / 80 °C 2: 43 percent / diisobutylaluminum hydride / toluene; hexane / 2 h / -68 °C View Scheme

2: 53 percent / chloramine T / dioxane; H2O / 1 h View Scheme

Yield given. Multistep reaction. Yields of byproduct given;