(+/-)-alpha-硫辛酰胺合成路线 (共 9 条)
反应条件
ammonium hydroxide in dichloromethane; acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
De La Reberdiere, Arnaud; Lachaud, Fabien; Chuburu, Francoise; Cadiou, Cyril; Lemercier, Gilles
Tetrahedron Letters, 2012 , vol. 53, # 45 p. 6115 - 6118,4
反应条件
oxidized dithiothreitol pH 7.0; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 102, # 6 p. 2011 - 2026
反应条件
tetrahydrofuran; triethylamine; isobutyl chloroformate Behandeln der Reaktionsloesung mit Ammoniak enthaltendem Tetrahydrofuran;
参考文献
Journal of Biological Chemistry, , vol. 232, p. 143,144
反应条件
in phosphate buffer; N,N-dimethyl-formamide T=30°C; Oxidation; Reduction; Product distribution; Further Variations:pH-valuesother quinones;
参考文献
Biochemical Pharmacology, , vol. 51, # 3 p. 275 - 283
反应条件
ethylenediaminetetraacetic acid in phosphate buffer T=30°C; pH=7.0; Enzyme kinetics;
参考文献
Chakraborty, Saikat; Sakka, Makiko; Kimura, Tetsuya; Sakka, Kazuo
Bioscience, Biotechnology and Biochemistry, 2008 , vol. 72, # 4 p. 982 - 988
反应条件
3,3'-tetramethylene-bridged 4-methylthiazolium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene in methanol 5 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 858 - 859
反应条件
triethyl borane; tributylphosphine; sodium hydrogencarbonate; triethyl phosphite in propan-1-ol 36 h; Ambient temperatureIrradiation;
参考文献
Cuesta, Javier; Arsequell, Gemma; Valencia, Gregorio; Gonzalez, Asensio
Tetrahedron Asymmetry, 1999 , vol. 10, # 14 p. 2643 - 2646
反应条件
DL-threo-1,4-dimercapto-2,3-butanediol
pH 7.0; Equilibrium constant;
参考文献
Szajewski, Richard P.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2011 - 2026
反应条件
3,3'-tetramethylene-bridged 4-methylthiazolium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene in methanol
5 h;
参考文献
Inoue, Hiroo; Tamura, Shigeo
Journal of the Chemical Society, Chemical Communications, 1986 , # 11 p. 858 - 859