1-甲基亚磺酰基-4-硝基苯合成路线 （共 11 条）
反应条件
sodium hydroxide in 1,4-dioxane; water T=50°C; ΔS(excit.), ΔH(excit.); Thermodynamic dataKinetics;
参考文献
Chisari, Alfio; Maccarone, Emanuele; Parisi, Giovanni; Perrini, Giancarlo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 957 - 960
反应条件
1.1: Heating 2.1: Et3N; EtOH 2.2: NH4Cl View Scheme
参考文献
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, , vol. 41, # 9 p. 1763 - 1766
反应条件
rhenic(VII) acid; benzo[1,3,2]dioxaborole in tetrahydrofuran T=20°C; 0.166667 h; chemoselective reaction;
参考文献
Cabrita, Ivania; Sousa, Sara C.A.; Fernandes, Ana C.
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6132 - 6135
反应条件
2,3-dimethylbutane-2,3-diol; [MoO2Cl2(dmf)2] in acetonitrile T=90°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 2-3 p. 321 - 327
反应条件
2,3-dimethylbutane-2,3-diol; [MoO2Cl2(dmf)2] in acetonitrile T=90°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 2-3 p. 321 - 327
反应条件
1: [MoO2Cl2(dmf)2]; 2,3-dimethylbutane-2,3-diol / acetonitrile / 8 h / 90 °C 2: [MoO2Cl2(dmf)2]; 2,3-dimethylbutane-2,3-diol / toluene / 0.33 h / 150 °C / Microwave irradiation View Scheme
参考文献
Garcia, Nuria; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Rubio, Ruben; Pedrosa, Maria R.; Arnaiz, Francisco J.; Sanz, Roberto
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 321 - 327
反应条件
1: With bis(acetylacetonate)oxovanadium; (R)-diiodo Shiff base ligand in chloroform T=22°C; 1 h; 2: With dihydrogen peroxide in chloroform T=22°C; 20 h; Title compound not separated from byproducts;
参考文献
Mohammadpoor-Baltork, Iraj; Hill, Mathias; Caggiano, Lorenzo; Jackson, Richard F. W.
Synlett, 2006 , # 20 p. 3540 - 3544
反应条件
phthalic anhydride; urea hydrogen peroxide in methanol 24 h; Ambient temperature;
参考文献
Compton, Richard G.; Dryfe, Robert A. W.; Eklund, John C.; Page, Stephen D.; Hirst, Judy; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 8 p. 1673 - 1678
反应条件
in acetone T=293°C; Kinetics; Further Variations:SolventsTemperatures;
参考文献
Hanson, Peter; Hendrickx, Ramon A. A. J.; Smith, John R. Lindsay
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 6 p. 762 - 771
反应条件
T=25°C; Rate constant;
参考文献
Cerniani; Modena
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 843,846
