in tetrahydrofuran
LiSnMe3 added to p-MeOC6H4SnEt3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Mochida, Kunio
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3299 - 3306
in tetrahydrofuran
byproducts: methoxybenzene; (4-methoxyphenyl)trimethylstannane dissolved in dry THF was cooled at -60°C; FClO3/N2 mixt. passed through soln. for about 35 min; soln. warmed up to ambient temp. under stirring and stirred at about 60°C for 20 min (closed conditions) or; isolated by semi-preparative thin-layer chromy. (silica gel 60, petroleum ether/ethyl acetate 10:1);
