N,N’-双亚水杨-1,2-丙二胺合成路线 (共 6 条)
反应条件
in methanol 1 h; Reflux;
参考文献
Li, Qing-Bin; Xue, Ling-Wei; Yang, Wei-Chun; Zhao, Gan-Qing
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013 , vol. 43, # 7 p. 822 - 825
反应条件
in ethanol T=20°C; Condensation; 2 h;
参考文献
Choudhary, Nosheen F.; Connelly, Neil G.; Hitchcock, Peter B.; Leigh, G. Jeffery
Journal of the Chemical Society - Dalton Transactions, 1999 , # 24 p. 4437 - 4446
参考文献
Iowa State College Journal of Science, , vol. 21, p. 110,116
反应条件
in not given prepn. according to general procedures see P. E. Riley et al., Inorg. Chem. 1986, 25, 154 and J. Selbin et al., J. Inorg. Nucl. Chem. 1963, 25, 1253; elem. anal.;
参考文献
Choudhary, Nosheen; Hughes, David L.; Kleinkes, Uwe; Larkworthy, Leslie F.; Leigh, G. Jeffery; Maiwald, Michael; Marmion, Celine J.; Sanders, J. Roger; Smith, Gallenius W.; Sudbrake, Claas
Polyhedron, 1997 , vol. 16, # 9 p. 1517 - 1528
反应条件
NaOAc * 3H2O in methanol; water addn. of aq. soln. of Cu-salt to methanolic soln. of ligand and reagent (pptn.), refluxing (stirring, 4 h); cooling to room temp., standing (0°C, 12 h), filtration, washing (H2O, MeOH), extn. (CHCl3), drying (vac., room temp. 72 h); elem. anal.;
参考文献
Felicio, Roberto C.; Da Silva, Gislaine A.; Ceridorio, Lucineia F.; Dockal, Edward R.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 2 p. 171 - 192
反应条件
in acetone mixed; cooled, concd., filtered, recrystd. (acetone); elem. anal.;
参考文献
Popova; Orlova; Shagisultanova
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 2000 , vol. 26, # 10 p. 686 - 689