反应条件
1: 1.) NaBH4/BF3*Et2O, 2.) 30percent H2O2/6M NaOH / 1.) diglyme, 20 deg C, 1h, 2.) diglyme, water, reflux, 1 h
2: 92 percent / Jones reagent / acetone / 1 h / 0 °C
3: 83 percent / acetic acid / Ambient temperature
4: 86 percent / 1M NaOH / H2O / 1 h / 10 °C
5: 100 percent / dioxane; diethyl ether
6: 95 percent / PDC / 1.) CH2Cl2, room temp., 12 h, 2.) CH2Cl2, Et2O, r.t., 2 h
View Scheme
参考文献
Barreiro, Eliazer J.; Costa, Paulo R. R.; Coelho, Fernando A. S.; Farias, Florence M. C. de
Journal of Chemical Research, Miniprint, 1985 , # 7 p. 2301 - 2332
