二环戊亚甲基二硫化四烷基秋兰姆合成路线 (共 27 条)
反应条件
in N,N-dimethyl-formamide 2 h; Heating;
参考文献
Ramadas; Srinivasan
Synthetic Communications, 1995 , vol. 25, # 21 p. 3381 - 3387
参考文献
Fromm
Chemische Berichte, 1909 , vol. 42, p. 1954
参考文献
Fromm
Chemische Berichte, 1909 , vol. 42, p. 1954
反应条件
1: With chlorine in dichloromethane T=24 - 26°C; 7.83333 h; Cooling with ice; 2: With water; sodium hydrogencarbonate in dichloromethane Cooling with ice;
参考文献
Adeppa; Rupainwar; Misra, Krishna
Synthetic Communications, 2011 , vol. 41, # 2 p. 285 - 290
反应条件
oxygen in isopropyl alcohol
T=50°C; P=1275.13 Torr; 0.5 h; Autoclave;
参考文献
Adeppa; Rupainwar; Misra, Krishna
Synthetic Communications, 2011 , vol. 41, # 2 p. 285 - 290
反应条件
sodium perchlorate in water
T=0 - 5°C; 0.25 h;
参考文献
Ramadas; Srinivasan
Synthetic Communications, 1995 , vol. 25, # 2 p. 227 - 234
反应条件
carbon tetrabromide in N,N-dimethyl-formamide
T=20°C; 2.5 h; Cooling with ice;
参考文献
Liang, Fushun; Tan, Jing; Piao, Chengri; Liu, Qun
Synthesis, 2008 , # 22 p. 3579 - 3584
反应条件
hydrogenchloride; sodium nitrite in methanol; water
T=0 - 5°C;
参考文献
Kapanda, Coco N.; Muccioli, Giulio G.; Labar, Geoffray; Poupaert, Jacques H.; Lambert, Didier M.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 22 p. 7310 - 7314
参考文献
Monsanto Chem. Co.
Patent: US2286690 , 1940 ;
反应条件
in benzene
T=0 - 5°C; Addition; Disproportionation;
参考文献
Boi, Luu Van
Russian Chemical Bulletin, 2000 , vol. 49, # 2 p. 335 - 343
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2000 , vol. 49, # 2 p. 334 - 342