3-苯基-N-(3-苯基丙基)-1-丙胺合成路线 (共 41 条)
反应条件
ethanol; sodium carbonate T=120°C;
反应条件
in dimethyl sulfoxide
T=20°C; 12 h;
参考文献
Zha, Congxiang; Brown, George B.; Brouillette, Wayne J.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 1 p. 95 - 104
反应条件
3 platinum on carbon; hydrogen in toluene
T=105°C; P=4500.45 Torr; Flow reactor;
参考文献
Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 85 - 88
反应条件
3 platinum on carbon; hydrogen in toluene
T=105°C; P=4500.45 Torr; Flow reactor;
参考文献
Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 85 - 88
反应条件
1: With titanium(IV) isopropylate; ammonium chloride; triethylamine in ethanol
T=20°C; 6 h;
2: With sodium tetrahydroborate in ethanol
T=20°C; 3 h; Further stages.;
参考文献
Miriyala, Bruhaspathy; Bhattacharyya, Sukanta; Williamson, John S.
Tetrahedron, 2004 , vol. 60, # 7 p. 1463 - 1471
反应条件
acetic acid ester; ethanol; nickel
Hydrogenation;
参考文献
Rupe; Glenz
Helvetica Chimica Acta, 1922 , vol. 5, p. 941
反应条件
diethyl ether; nickel
T=100°C; Hydrogenation.unter Druck;
参考文献
Winans; Adkins
Journal of the American Chemical Society, 1933 , vol. 55, p. 2051,2056
Full Text Show Details
Winans; Adkins
Journal of the American Chemical Society, 1932 , vol. 54, p. 306,311
Journal of the American Chemical Society, 1933 , vol. 55, p. 2051,2056, 2057
反应条件
NH4BF4; sodium hydrogencarbonate; [{(η5-C5Me5)IrCl}2(μ-Cl)2]
T=140°C; 17 h;
参考文献
Yamaguchi, Ryohei; Kawagoe, Shoko; Asai, Chiho; Fujita, Ken-Ichi
Organic Letters, 2008 , vol. 10, # 2 p. 181 - 184
反应条件
sodium tris(acetoxy)borohydride in 2-methyl tetrahydrofuran
T=18°C; 24 h; Green chemistry; SolventReagent/catalyst;
参考文献
McGonagle, Fiona I.; MacMillan, Donna S.; Murray, Jane; Sneddon, Helen F.; Jamieson, Craig; Watson, Allan J. B.
Green Chemistry, 2013 , vol. 15, # 5 p. 1159 - 1165
反应条件
dimethylammonium chloride in acetic acid
T=115°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Manninen, Kalle; Karjalainen, Aira
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 3 p. 190 - 195