反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1781585', constants.ctx, '0')">diethyl 1,2-hydrazinedicarboxylate</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br /> cooling; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1697908', constants.ctx, '0')">3-bromo-2-methylprop-1-ene</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=20 - 80°C; 4.5 h; <br />
参考文献
Markovic, Dean; Varela-Alvarez, Adrian; Sordo, Jose Angel; Vogel, Pierre Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 7782 - 7795