5-乙基-3,8-二硝基-6-苯基菲啶鎓乙基硫酸盐合成路线 （共 6 条）
反应条件
1: With sulfuric acid; iron in ethanol; water 1.5 h; Reflux; 2: With ammonia in ethanol; water T=25°C; Further stages;
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
反应条件
1: nitric acid / tetrachloromethane
2: hydrogen / ethanol / 60 °C / 22052.2 Torr
3: sulfuric acid; potassium nitrate
4: tin(IV) chloride / nitrobenzene
5: nitrobenzene / 17.5 h / 20 - 165 °C
View Scheme
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
反应条件
1: hydrogen / ethanol / 60 °C / 22052.2 Torr
2: sulfuric acid; potassium nitrate
3: tin(IV) chloride / nitrobenzene
4: nitrobenzene / 17.5 h / 20 - 165 °C
View Scheme
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
反应条件
1: tin(IV) chloride / nitrobenzene
2: nitrobenzene / 17.5 h / 20 - 165 °C
View Scheme
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
反应条件
1: sulfuric acid; potassium nitrate
2: tin(IV) chloride / nitrobenzene
3: nitrobenzene / 17.5 h / 20 - 165 °C
View Scheme
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
反应条件
in nitrobenzene
T=20 - 165°C; 17.5 h;
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
