2,2,2-三甲基苯乙酮合成路线 (共 203 条)
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Tetrahedron Letters, , vol. 25, # 42 p. 4805 - 4808
反应条件
in tetrahydrofuran T=-78°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 10 p. 1885 - 1888
反应条件
1: n-bityllithium / hexane; diethyl ether / 1.) 30 min, 0-5 deg C; 2.) 6 h, 25 deg C 2: various solvent(s); 1,2-dimethoxy-ethane / 72 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, p. 4494
反应条件
ammonium chloride in tetrahydrofuran T=-78°C; 0.25 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 358 - 359
反应条件
N,N,N',N,-tetramethylethylenediamine; sodium; lithium in tetrahydrofuran T=15 - 18°C; 0.25 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 60, # 1 p. 8 - 9
反应条件
naphthalene; lithium in tetrahydrofuran T=0 - 20°C; Alkylation; 0.416667 h;
参考文献
Journal of Organic Chemistry, , vol. 61, # 17 p. 6058 - 6059
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Journal of Organic Chemistry, , vol. 78, # 11 p. 5273 - 5281
反应条件
water in acetone T=25°C; 2 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, # 10 p. 1822 - 1828
Zhurnal Organicheskoi Khimii, , vol. 18, # 10 p. 2071 - 2077
反应条件
dicarbonic acid,dimethyl ester; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 6 h;
参考文献
Chemistry Letters, , # 12 p. 1242 - 1243
反应条件
iron (III) acetylacetonate in tetrahydrofuran 0.166667 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 25, # 42 p. 4805 - 4808