3,3’,4,4’-四溴联苯醚合成路线 (共 5 条)
反应条件
1,4-dioxane dibromide T=100°C;
参考文献
Tolstaya, T. P.; Vanchikova, L. N.; Lisichkina, I. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 6 p. 1282 - 1285
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 6 p. 1392 - 1395
参考文献
Chen; Konstantinov; Chittim; Joyce; Bols; Bunce
Environmental Science and Technology, 2001 , vol. 35, # 18 p. 3749 - 3756
反应条件
1: 45 percent / NaOH / H2O 2: 95 percent / Br2; iron powder / CH2Cl2 / 2 h / 50 °C View Scheme
参考文献
Environmental Science and Technology, , vol. 33, # 17 p. 3033 - 3037
反应条件
1.1: TFA; NaNO2 / 0 °C 1.2: 65 percent / aq. Na2SO4; H2SO4 / 0.83 h / Heating 2.1: 87 percent / aq. NaOH View Scheme
参考文献
Environmental Science and Technology, , vol. 35, # 18 p. 3749 - 3756
反应条件
1: HBr (con.), NaNO2 2: 34 percent / Cu2Br2, HBr (con.) 3: 82 percent / dioxane dibromide / 100 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 6 p. 1282 - 1285
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1392 - 1395