1: 93.5 percent / PCl5 / various solvent(s) / 4 h / Heating 2: H2; NaOAc / Pd/C / H2O; ethanol View Scheme

phosphorus pentachloride in various solvent(s) Substitution; 4 h; Heating;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4267587', constants.ctx, '0')">potassium carbonate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br /> <br /> <br /> &nbsp;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />2&nbsp;h;&nbsp;&nbsp;Heating;&nbsp;<br /> &nbsp;