1-(苯基硫代)丙烷-2-醇合成路线 (共 33 条)
反应条件
α-n-hexadecene; Corynebacterium equi in water T=30°C; 168 h; pH 8;
参考文献
Ohta, Hiromichi; Kato, Yasuo; Tsuchihashi, Gen-ichi
Chemistry Letters, 1986 , p. 581 - 584
反应条件
1: 50 percent / 168 h / 30 °C / corynebacterium equi IFO 3730 2: 99 percent / Na2WO4, cetyltrimethylammoniu chloride, 35percent hydrogen peroxide / CH2Cl2 / 24 h / Ambient temperature View Scheme
参考文献
Ohta, Hiromichi; Kato, Yasuo; Tsuchihashi, Gen-ichi
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2735 - 2739
反应条件
pyridine; trichlorophosphate
参考文献
GRUeNENTHAL GMBH
Patent: US2010/234429 A1, 2010 ;
Location in patent: Page/Page column 20 ;
反应条件
T=118 - 189°C; effective rate constants of the exchange reaction; Rate constant;
参考文献
Malievskii, A. D.; Vints, V. V.; Kalugina, I. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 2 p. 267 - 273
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 2 p. 293 - 300
反应条件
1: 50 percent / 168 h / 30 °C / corynebacterium equi IFO 3730 2: 97 percent / perbenzoic acid / CHCl3 / 1 h / 0 °C View Scheme
参考文献
Ohta, Hiromichi; Kato, Yasuo; Tsuchihashi, Gen-ichi
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2735 - 2739
反应条件
pyridine T=0 - 20°C; Inert atmosphere;
参考文献
Gariani, Rogerio A.; Luengo, Fernando A.G.; Vale, Luiz A.S.; Bazito, Reinaldo C.; Comasseto, Joao V.
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3336 - 3338
反应条件
sodium tetrahydroborate in methanol
T=0°C; 3 h;
参考文献
Watanabe, Mikio; Nakamori, Seijin; Hasegawa, Hatsue; Shirai, Kozo; Kumamoto, Takanobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 817 - 821
反应条件
hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 0.333333 h; regioselective reaction;
参考文献
Ganesh, Venkataraman; Chandrasekaran, Srinivasan
Synthesis, 2009 , # 19 p. 3267 - 3278
反应条件
in water
T=20°C; 0.25 h; Solvent; regioselective reaction;
参考文献
Propersi, Simona; Tidei, Caterina; Bagnoli, Luana; Marini, Francesca; Testaferri, Lorenzo; Santi, Claudio
Journal of Sulfur Chemistry, 2013 , vol. 34, # 6 p. 671 - 676
反应条件
magnesium oxide; copper
T=20°C; 0.5 h; chemoselective reaction;
参考文献
Das, Biswanath; Balasubramanyam, Penagaluri; Krishnaiah, Maddeboina; Veeranjaneyulu, Boyapati; Sudhakar, Dega
Synthetic Communications, 2010 , vol. 40, # 14 p. 2113 - 2121