N-(1-环戊烯基)吗啉合成路线 (共 77 条)
反应条件
1: Et3N / CHCl3 / 1 h 2: 46.9 percent / H2 / Adams' PtO2 / 0.5 h 3: 60 percent / H2 View Scheme
参考文献
Zhang, Pang; Li, Lian-chu
Synthetic Communications, 1986 , vol. 16, # 8 p. 957 - 966
反应条件
1: 70 percent / Et3N / CHCl3 / 0.5 h 2: 79 percent / H2 / Adams' platinum oxide / ethanol / 0.5 h 3: 79 percent / Heating 4: 97 percent / H2 View Scheme
参考文献
Zhang, Pang; Li, Lian-chu
Synthetic Communications, 1986 , vol. 16, # 8 p. 957 - 966
反应条件
zinc in diethyl ether
参考文献
Senoez, Huelya; Tunoglu, Nazan
Chemical and Pharmaceutical Bulletin, 2003 , vol. 51, # 4 p. 444 - 447
反应条件
1: in acetonitrile Heating; 2: With water Heating; Further stages.;
参考文献
Ishibashi; Kobayashi; Nakashima; Tamura
Journal of Organic Chemistry, 2000 , vol. 65, # 26 p. 9022 - 9027
反应条件
1: With triethylamine Heating; 2: With hydrogenchloride Heating; 3: With potassium hydroxide T=100°C;
参考文献
Bell, Roel P.L.; Verdijk, Dennis; Relou, Mike; Smith, Dennis; Regeling, Henk; Ebbers, Eelco J.; C. Leemhuis, Frank M.; Oniciu, Daniela C.; Cramer, Clay T.; Goetz, Brian; Pape, Michael E.; Krause, Brian R.; Dasseux, Jean-Louis
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 223 - 236
反应条件
hydrogenchloride in diethyl ether; butan-1-ol; benzene
参考文献
May and Baker Limited
Patent: US4171375 A1, 1979 ;
反应条件
(i) cyclohexane, (ii) aq. HCl, nBuOH; Multistep reaction;
参考文献
Burton; Caton; Coffee; Parker; Stuttle; Watkins
Journal of the Chemical Society. Perkin transactions 1, 1976 , # 23 p. 2550 - 2556
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane Heating;
参考文献
South, Michael S.; Jakuboski, Terri L.; Westmeyer, Mark D.; Daniel
Journal of Organic Chemistry, 1996 , vol. 61, # 25 p. 8921 - 8934
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Katsin,N.; Ikan,R.
Synthetic Communications, 1977 , vol. 7, p. 185 - 188
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Katsin,N.; Ikan,R.
Synthetic Communications, 1977 , vol. 7, p. 185 - 188