2,2,6,6-四甲基哌啶盐酸盐合成路线 （共 4 条）
反应条件
in toluene
byproducts: Me3SiCl; under protective gas; reflux of solution (10 h);; evapn. (vacuo); extn. (n-hexane/CH2Cl2); residue was recrystd. (CH2Cl2); elem. anal.; extract contains mixture of two B-compounds; (11)B-NMR;;
参考文献
Einholz, Wolfgang; Frey, Gerhard; Haubold, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 1 p. 47 - 54
反应条件
hydrogenchloride in 1,4-dioxane
Inert atmosphere;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813
反应条件
sulfuryl dichloride in chloroform-d1
Inert atmosphere; Solvent;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813
反应条件
in methanol; benzene
3 h; Irradiation;
参考文献
Carloni; Carloni, Patricia; Damiani; Damiani, Elisabetta; Iacussi; Iacussi, Marco; Greci; Greci, Lucedio; Stipa; Stipa, Pierluigi; Cauzi; Cauzi, Daniele; Rizzoli; Rizzoli, Corrado; Sgarabotto; Sgarabotto, Paolo
Tetrahedron, 1995 , vol. 51, # 45 p. 12445 - 12452
