Merck
Patent: DE238959 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 1313
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v. Braun
Chemische Berichte, 1910 , vol. 43, p. 2847
2-[(N,N-diisopropylamino)methyl]phenylboronic acid in o-di-fluorobenzene
T=85°C; 48 h; KineticsProduct distribution; Further Variations:CatalystsSolventsTemperaturesthermal reaction without catalyst;
参考文献
Arnold, Kenny; Davies, Bryan; Giles, Richard L.; Grosjean, Christophe; Smith, Gillian E.; Whiting, Andrew
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 7-8 p. 813 - 820
1: nitric acid / -15 °C
2: tin dichloride; concentrated hydrochloric acid; alcohol
3: durch Diazotieren in schwefelsaurer Loesung und folgendes Verkochen der Diazoniumsalz-Loesung
4: hydrochloric acid (20 percent ) / 135 - 140 °C / im Einschlussrohr
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参考文献
v.Braun
Chemische Berichte, 1914 , vol. 47, p. 495
