(1R,2R,6S,7S)-三环[5.2.1.02,6]癸-3,8-二烯合成路线 （共 14 条）
反应条件
1: 80 percent / H2, Raney Nickel / 48 h / 228000 Torr 2: 80 percent / SeO2, acetic anhydride / H2O / 96 h / Ambient temperature View Scheme
参考文献
Kazennova, N. B.; Shestakova, A. K.; Chertkov, V. A.; Ustynyuk, N. A.; Ustynyuk, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 10 p. 1889 - 1891
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 10 p. 2108 - 2111
反应条件
C54H81ClP3Rh in dichloromethane T=90°C; 3 h; Under argonSealed;
参考文献
Khusnutdinov; Shchadneva; Mukhametshina
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 1 p. 54 - 58
反应条件
T=170°C; 3 h; var. reaction time and temperature; Product distributionMechanism;
参考文献
Mamedov
Russian Journal of Nondestructive Testing, 1997 , vol. 33, # 2 p. 165 - 168
反应条件
C54H81ClP3Rh in dichloromethane T=90°C; 3 h; Under argonSealed;
参考文献
Khusnutdinov; Shchadneva; Mukhametshina
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 1 p. 54 - 58
反应条件
T=170°C; 3 h; var. reaction time and temperature; Product distributionMechanism;
参考文献
Mamedov
Russian Journal of Nondestructive Testing, 1997 , vol. 33, # 2 p. 165 - 168
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Mamedov, M. K.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 4 p. 485 - 488
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 4 p. 528 - 534
反应条件
sodium hydroxide; toluene-4-sulfonic acid 1.) 100 deg C, 5 h, 2.) 40 deg C, 2 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Mamedov, M. K.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 4 p. 485 - 488
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 4 p. 528 - 534
反应条件
toluene-4-sulfonic acid T=140°C; 5 h; Title compound not separated from byproducts;
参考文献
Mamedov
Russian Journal of Nondestructive Testing, 1997 , vol. 33, # 2 p. 165 - 168
反应条件
toluene-4-sulfonic acid
T=140°C; 5 h; Title compound not separated from byproducts;
参考文献
Mamedov
Russian Journal of Nondestructive Testing, 1997 , vol. 33, # 2 p. 165 - 168
反应条件
hydrogenchloride
T=200°C; 0.5 h;
参考文献
Gataullin; Kazhanova; Sagitdinov; Galyautdinov; Fatykhov; Spirikhin; Abdrakhmanov
Russian Journal of Applied Chemistry, 2001 , vol. 74, # 2 p. 280 - 285
