顺-3,3,5-三甲基环己醇合成路线 （共 24 条）
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; trans-3,3,5-trimethylcyclohexanone; zirconium tetra-n-propoxide in dichloromethane T=20°C; 7 h;
参考文献
Krohn, Karsten; Vinke, Ingeborg; Adam, Horst
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1467 - 1472
反应条件
lithium tert-butoxymagnesium hydride in tetrahydrofuran
Ambient temperature;
参考文献
Ashby, Eugene C.; Noding, Stephen A.; Goel, Anil B.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1028 - 1035
反应条件
4,4'-di-tert-butylbiphenyl; lithium; iron(II) chloride in tetrahydrofuran
T=20°C; 5 h;
参考文献
Moglie, Yanina; Alonso, Francisco; Vitale, Cristian; Yus, Miguel; Radivoy, Gabriel
Tetrahedron, 2006 , vol. 62, # 12 p. 2812 - 2819
反应条件
hydrogenchloride; K9-OThx-9-BBNH) in tetrahydrofuran
T=0°C; stereoselectivity, other boranes; Product distribution;
参考文献
Brown, Herbert C.; Cha, Jin Soon; Nazer, Behrooz
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2073 - 2074
反应条件
sodium tetrahydroborate; N-hexadecyl-N,N-bis(2-hydroxyethyl)-N-methylammonium bromide in water; toluene
T=20°C; 20 h; Yields of byproduct given;
参考文献
D'Incan, E.; Loupy, A.
Tetrahedron, 1981 , vol. 37, p. 1171 - 1180
反应条件
hydrogen; palladium on activated charcoal in ethanol
P=760 Torr; 1 h; Ambient temperature;
参考文献
Crabtree, Robert H.; Davis, Mark W.
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2655 - 2661
反应条件
hydrogenchloride in ethanol
3 h; Heating;
参考文献
Schaper, Ulf-Armin
Synthesis, 1981 , # 10 p. 794 - 796
反应条件
2,5-dimethyl-2,5-dihydroxy hexane; nickel diacetate; sodium hydride; magnesium bromide in tetrahydrofuran
T=63°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Feghouli, G.; Vanderesse, R.; Fort, Y.; Caubere, P.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1383 - 1384
反应条件
tetra-N-butylammonium borohydride in toluene
T=95°C; 20 h; Yield given;
参考文献
D'Incan, E.; Loupy, A.
Tetrahedron, 1981 , vol. 37, p. 1171 - 1180
反应条件
nickel
T=130°C; P=5148.6 Torr; Hydrogenation;
参考文献
Peppiatt; Wicker
Journal of the Chemical Society, 1955 , p. 3122
