4-(1-吡咯烷)-1-丁醇合成路线 （共 11 条）
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Eli Lilly and Company
Patent: US6025382 A1, 2000 ;
反应条件
hydrogen in ethylene glycol dimethyl ether T=160°C; P=22502.3 Torr; 20 h; Inert atmosphereAutoclaveMolecular sieve;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 8 p. 2231 - 2234
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 22, p. 122,125
反应条件
aluminum oxide T=260°C;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 239, p. 889
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 4 p. 297 - 302
反应条件
1: 43 percent / TiCl4 / CH2Cl2 / 3 h / 0 °C 2: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 4 p. 297 - 302
反应条件
ammonia; hydrogen; iron RFC T=260°C; other temp. (280, 300, 310 deg C); Product distributionMechanism;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 2 p. 161 - 164
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 23, # 2 p. 195 - 198
反应条件
triphenylphosphine; ruthenium trichloride T=120°C; 15 h; other catalyst, also with THF, other phosphine, also at 220 degC; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 343 - 352
反应条件
1: Raney nickel; ethanolic KOH-solution / Hydrogenation 2: aluminium oxide / 260 °C View Scheme
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 239, p. 889
参考文献
Journal of Organic Chemistry, , vol. 14, p. 862,866
Org. Synth. Coll., , vol. Vol. IV, p. 834
