3-乙酰基-1-甲基吡咯合成路线 （共 10 条）
反应条件
tetrabutylammomium bromide; potassium carbonate in butanone T=60°C; 12 h;
参考文献
Croce, Piero Dalla; Ferraccioli, Rafaella; Ritieni, Alberto
Synthesis, 1990 , # 3 p. 212 - 213
反应条件
1: N-methyl-hydroxylamine hydrochloride; dimethyl acetylenedicarboxylate With potassium hydrogencarbonate in dichloromethane 0.25 h; 2: acetyl chloride in dichloromethane T=40°C; 3 h;
参考文献
Valizadeh, Hassan; Fakhari, Ashraf
Molecules, 2010 , vol. 15, # 5 p. 2972 - 2979
反应条件
palladium on activated charcoal T=210°C;
参考文献
Anderson, Hugh J.; Loader, Charles E.; Foster, Aidan
Canadian Journal of Chemistry, 1980 , vol. 58, p. 2527 - 2530
反应条件
ethylaluminum dichloride in dichloromethane T=0°C;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 46 p. 8030 - 8035
反应条件
trifluoroacetic acid T=72°C; 1.5 h; Mechanism;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
反应条件
4-(N,N-dimethlyamino)pyridine 1.) MeCN, 15 min, 2.) CD3CN, D2O, 95-100 deg C, 50 min; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2125 - 2146
反应条件
1: Oxonereg; / methanol / 12 h / 20 °C 2: sodium hydroxide / water / 2.5 h / 20 °C 3: trichlorophosphate / 1,2-dichloro-ethane View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 50, # 4 p. 795 - 808
反应条件
1: sodium hydroxide / water / 2.5 h / 20 °C 2: trichlorophosphate / 1,2-dichloro-ethane View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 50, # 4 p. 795 - 808
反应条件
1: With trichlorophosphate in 1,2-dichloro-ethane Vilsmeier-Haack Formylation; 2: With sodium acetate in water Vilsmeier-Haack Formylation;
参考文献
Journal of Heterocyclic Chemistry, , vol. 50, # 4 p. 795 - 808
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in tetrahydrofuran Ambient temperature;
参考文献
Synthesis, , # 3 p. 212 - 213
