反应条件
in diethyl ether stirring, warming from -78°C to ambient temp.; cooling to -30°C yields one enantiomer (filtn., drying in vacuo), cooling to -78°C or evaporation of mother liquor yields mixtures of enantiomers, which could be sepd. by repeated recrystn. from hexane and/or diethyl ether; elem. anal.;
参考文献
Angermund, Hildegard; Grevels, Friedrich-Wilhelm; Moser, Rainer; Benn, Reinhard; Krueger, Carl; Romao, Maria J.
Organometallics, 1988 , vol. 7, p. 1994 - 2004
