1: cyclohexylacetylene With n-butyllithium in diethyl ether; hexane
T=-78°C; 1 h;
2: carbon dioxide in hexane; dichloromethane
T=-78 - 20°C;
参考文献
Alhamadsheh, Mamoun M.; Palaniappan, Nadaraj; DasChouduri, Suparna; Reynolds, Kevin A.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1910 - 1911
1: cyclohexylacetylene With n-butyllithium in tetrahydrofuran; hexanes
T=-78°C; 0.833333 h; Inert atmosphere;
2: 2,4,6-trimethyl-1,3,5-trioxane T=-78 - 23°C; Inert atmosphere;
参考文献
Worthy, Amanda D.; Joe, Candice L.; Lightburn, Thomas E.; Tan, Kian L.
Journal of the American Chemical Society, 2010 , vol. 132, # 42 p. 14757 - 14759
diisopropylamine; copper(I) bromide in 1,4-dioxane
7 h; Heating;
参考文献
Searles, Scott; Li, Yushun; Nassim, Bahman; Lopes, Maria-Teresa Robert; Tran, P. T.; Crabbe, Pierre
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 747 - 751
