2-乙氧基-4,5-二氢-3H-吡咯合成路线 (共 5 条)
反应条件
1: 96 percent / HCl gas / diethyl ether / 0.08 h 2: 88 percent / H2O / 10 h / Ambient temperature View Scheme
参考文献
Menezes, Royce; Smith, Michael B.
Synthetic Communications, 1988 , vol. 18, # 4 p. 1625 - 1636
反应条件
in dichloromethane
4 h; Heating;
参考文献
Kuehne, Paul; Linden, Anthony; Hesse, Manfred
Helvetica Chimica Acta, 1996 , vol. 79, # 4 p. 1085 - 1094
反应条件
T=60 - 100°C; Etherification; 15 h;
参考文献
Sheu, Jennline; Smith, Michael B.; Oeschger, Thomas R.; Satchell, Jacqueline
Organic Preparations and Procedures International, 1992 , vol. 24, # 2 p. 147 - 158
参考文献
CEPHALON, INC.; CEPHALON FRANCE; BACON, Edward R.; BAILEY, Thomas; CHATTERJEE, Sankar; DUNN, Derek; HOSTETLER, Greg A.; HUDKINS, Robert L.; LESUR, Brigitte; SUNDAR, Babu G.; YUE, Christophe; ZULLI, Allison L.
Patent: WO2011/2984 A1, 2011 ;
Location in patent: Page/Page column 26 ;
WO 2011/002984 A1
反应条件
bis(acetylacetonate)nickel(II)
T=100°C; Overnight;
参考文献
Brunerie, Pascal; Celerier, Jean-Pierre; Petit, Huguette; Lhommet, Gerard
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1183 - 1188