反应条件
1: 44.5 percent / conc.HCl / methanol / 0.17 h / 100 °C
2: 39.4 percent / aq.KOH / methanol / 3 h / Ambient temperature
3: 1.) LiAlH4, 2.) DDQ / 1.) benzene, ether, reflux, 30 min, 2.) dioxane, room temperature, 40 h
4: 81.3 percent / pyridine / 18.5 h
5: 83.8 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
6: 10 percent / trimethyl orthoformate, O2, toluene-p-sulphonic acid / dioxane
7: 39.8 percent / ethanol / 2.5 h / Irradiation
8: 75 percent / H2 / Pd-CaCO3 / pyridine
9: 28.5 mg / potassium hydrogen carbonate, H2O / ethanol / 1 h / Heating
10: 28 mg / HCl / 18 h / Ambient temperature
11: POCl3-pyridine
12: 60percent acetic acid / 91 h / Ambient temperature
13: 1 mg / H2 / Pd-C / dioxane / 6 h
View Scheme
参考文献
Cooley, George; Kirk, David N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 6 p. 1205 - 1212