1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
[cmmim][Cl] T=60 - 65°C; 1.6 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 11 p. 4517 - 4519
反应条件
1: in [D8]THF T=25°C; 2: With AcOH-d4 in [D8]THF
参考文献
Chemistry - A European Journal, , vol. 16, # 34 p. 10474 - 10481
参考文献
Tetrahedron Letters, , vol. 22, # 13 p. 1171 - 1174
反应条件
1: Diisopropylamine, butyllithium / THF, -78 deg C; 1.) 50 min, 2.) 5 min 2: 74 percent / 1. DMSO/oxalyl chloride; 2.(C2H5)3N / CH2Cl2 / 0.33 h / -60 °C View Scheme
参考文献
Synthesis, , # 7 p. 567 - 570
反应条件
1: 81 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 2: base / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 13 p. 1171 - 1174
反应条件
in tetrahydrofuran; hexane T=-78°C; 0.0833333 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 3 p. 698 - 705
反应条件
tetrabutyl ammonium fluoride; water in methanol 4 h; Reflux;
参考文献
Green Chemistry, , vol. 13, # 11 p. 3218 - 3223
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.; Pombo-Villar, Esteban
Tetrahedron Letters, 2002 , vol. 43, # 16 p. 2945 - 2948
反应条件
1: tetrahydrofuran 2: 85 percent / 2.) dil. HCl / dimethylformamide / 4 h / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 10 p. 2762 - 2768
反应条件
1: 83 percent / 1.) 1N NaOH, 2.) cc. HCl / H2O / Ambient temperature 2: tetrahydrofuran 3: 85 percent / 2.) dil. HCl / dimethylformamide / 4 h / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 10 p. 2762 - 2768
