1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
1: 1) NaHCO3 / 1) EtOH, rt, 10 min, 2) toluene, reflux, 2 h
2: C2H5ONa / ethanol / 1) rt, 15 min, 2) reflux, 2 h
View Scheme
参考文献
Abdalla; Sowell Sr.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1201 - 1207
反应条件
bromo-dimethylsulfonium bromide in dichloromethane
T=20°C; 0.333333 h;
参考文献
Khan, Abu T.; Ali, Md. Ashif; Goswami, Papori; Choudhury, Lokman H.
Journal of Organic Chemistry, 2006 , vol. 71, # 23 p. 8961 - 8963
反应条件
bromine in acetic acid
T=20°C; 0.0166667 h;
参考文献
Choi, Han Young; Chi, Dae Yoon
Organic Letters, 2003 , vol. 5, # 4 p. 411 - 414
反应条件
ammonium cerium (IV) nitrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen in ethyl acetate
T=60°C; P=760.051 Torr; 1 h; Schlenk techniqueMolecular sieve;
参考文献
Feng, Peng; Sun, Xiang; Su, Yijin; Li, Xinyao; Zhang, Li-He; Shi, Xiaodong; Jiao, Ning
Organic Letters, 2014 , vol. 16, # 12 p. 3388 - 3391
反应条件
ammonia; KNH2
anschliessendes Behandeln mit Benzaldehyd;
参考文献
Hauser; Harris
Journal of the American Chemical Society, 1958 , vol. 80, p. 6360,6363
反应条件
diboron trioxide; B(OsBu)3 in ethyl acetate
Condensation; 1 h;
参考文献
Venugopalan, P.; Krishnankutty, K.
Journal of the Indian Chemical Society, 1998 , vol. 75, # 2 p. 98 - 99
反应条件
tin(IV) chloride in benzene
24 h; Ambient temperature;
参考文献
Veronese, A. C.; Gandolfi, V.; Basato, M.; Corain, B.
Journal of Chemical Research, Miniprint, 1988 , # 8 p. 1843 - 1870
参考文献
Knorr; Lange
Chemische Berichte, 1902 , vol. 35, p. 3004
反应条件
sodium acetate; acetic acid
参考文献
Knorr; Lange
Chemische Berichte, 1902 , vol. 35, p. 3004
反应条件
sodium hydroxide; dihydrogen peroxide
T=0 - 20°C;
参考文献
Sheibani, Hassan; Islami, Mohammad Reza; Hassanpour, Avid; Saidi, Kazem
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 1 p. 13 - 20
