1-苯基-1,3-丁二酮合成路线 （共 471 条）
反应条件
acetic acid ester; diethyl ether; sodium amide
参考文献
Chemische Berichte, , vol. 38, p. 706
反应条件
ammonium hydroxide in acetonitrile
参考文献
Journal of Organic Chemistry, , vol. 51, # 10 p. 1692 - 1700
反应条件
1: acetophenone With lithium hexamethyldisilazane in tetrahydrofuran 0.25 h; 2: 2-oxopropionitrile in tetrahydrofuran
参考文献
Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.; Pombo-Villar, Esteban
Tetrahedron Letters, 2002 , vol. 43, # 16 p. 2945 - 2948
反应条件
L-proline T=20°C; 30 h;
参考文献
Shen, Zongxuan; Li, Bin; Wang, Lu; Zhang, Yawen
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8785 - 8788
反应条件
hydrogenchloride; water in dichloromethane T=20°C; 48 h;
参考文献
Sibgatulin, Dmitry A.; Volochnyuk, Dmitry M.; Kostyuk, Aleksander N.; Ivonin, Sergey P.; Lapandin, Andriy V.
Monatshefte fur Chemie, 2009 , vol. 140, # 6 p. 639 - 643
反应条件
hydrogenchloride; water in dichloromethane T=20°C; 48 h;
参考文献
Sibgatulin, Dmitry A.; Volochnyuk, Dmitry M.; Kostyuk, Aleksander N.; Ivonin, Sergey P.; Lapandin, Andriy V.
Monatshefte fur Chemie, 2009 , vol. 140, # 6 p. 639 - 643
反应条件
potassium tert-butylate in tert-butyl alcohol T=20°C; 3 h; Inert atmosphere;
参考文献
Nakaiida, Shoho; Kato, Shinzi; Niyomura, Osamu; Ishida, Masaru; Ando, Fumio; Koketsu, Jugo
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 5-6 p. 930 - 946
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; cataCXium®A; caesium carbonate T=60°C; P=2250.23 Torr; 36 h; GloveboxInert atmosphereAutoclave; Reagent/catalystSolventTemperaturePressureTime;
参考文献
Schranck, Johannes; Tlili, Anis; Alsabeh, Pamela G.; Neumann, Helfried; Stradiotto, Mark; Beller, Matthias
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12624 - 12628
反应条件
hydrogenchloride T=80°C; 1 h;
参考文献
Datta; Ila; Junjappa
Synthesis, 1988 , vol. 1, # 3 p. 248 - 250
反应条件
hydrogenchloride in N,N-dimethyl-formamide 4 h; Ambient temperature;
参考文献
Ohta, Shunsaku; Tsujimura, Atsuhiko; Okamoto, Masao
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2762 - 2768
