反应条件
in neat (no solvent)
byproducts: tributyltin malonate; addn. of ketone to organotin compd., equimolar ratio of educts, 96h, 200°C, distn. under reduced press., acidolysis by addn. of stoich. amt. of malonic acid in ether, reflux, 48h, ether removed, pptn. of malonate by addn. of pentane, under Ar; fractionated distn., alcohols detected by NMR, IR and chromy.;
参考文献
Daude, Gerard; Pereyre, Michel
Journal of Organometallic Chemistry, 1980 , vol. 190, # 1 p. 43 - 52
